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NMR Cryogen Fill Tips
Superconducting magnets
require liquid nitrogen (N2) and liquid Helium (He). Because it is difficult
to make a perfect dewar to hold these cryogens, they need to be periodically
replenished.
- Liquid nitrogen is
typically filled every 7 to 10 days and depending on your type of magnet,
liquid helium fills can be required as often as once a month to as infrequently
as only once or twice per year.
- Cryogen fills must
be performed correctly to avoid injury to you and the magnet.
- Injury to a magnet
could include breaking a seal on a dewar or quenching a magnet.
- Both forms of magnet
injuries are repairable, but at the least entail recharging the magnet;
at the most, they can entail replacing the magnet.
The following steps should
be observed:
- When filling the magnet
with liquid nitrogen, you must be sure not to exceed the recommended fill
pressure and rate for your magnet.
- If your magnet has
two liquid nitrogen ports, one should be used for filling and the other
for venting the boil-off gaseous nitrogen and overfill liquid nitrogen.
- A piece of tubing
is typically placed on the vent port to direct the overfill liquid nitrogen
away from the magnet seals, probe, and electronics.
- It is highly recommended
that your liquid nitrogen tanks be made of non-magnetic stainless steel.
- Liquid helium fills
are typically a awkward operation. Because they are done so infrequently,
it is good to review the process before each fill.
- The fill requires
a supply dewar of liquid helium, a special liquid helium transfer line,
and a tank of pure compressed helium gas.
- Liquid helium is transferred
from the liquid helium supply dewar up through the transfer line, into
the helium dewar of the magnet.
- The transfer line
goes into the top of the liquid helium supply dewar, but should never rest
on the bottom of the dewar.
- The bottom of the
dewar may contain frozen water, oxygen, and nitrogen which will be forced
into your magnet if the transfer line touches the bottom during the transfer
process.
- The compressed helium
gas, mentioned earlier, is for pressurizing the liquid helium supply dewar
with about 2 to 4 psi of pressure.
- Gauges on helium supply
dewars can be very inaccurate, so do not count on them to give you an accurate
reading.
- A helium pressure
above the liquid forces the Helium into the magnet dewar.
- The transfer line
is usually inserted into the magnet until it contacts a transfer flange
in the bottom of the magnet.
- The nitrogen ports
on the magnet should be plugged with a check valve during filling of the
helium dewar of the magnet.
- This step prevents
cryopumping, a process whereby nitrogen, water, and oxygen are condensed
out of the atmosphere into the nitrogen dewar due to the magnet stacks
being cooled by the helium.
- Many labs loosely
plug the helium vents with tissue during the fill. This cuts down on cryopumping
should the flow of the venting He drop.
- The best way to determine
if the magnet is full is to look for a change in the gas cloud coming out
of the magnet vents.
- When the magnet is
full the cloud becomes very thick with a deep white center plume with a
slight blue tint.
- The helium vents on
the magnet should be closed promptly after the magnet is full.
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